
Manual Kinematic Viscosity Bath with Glass Capillary Viscometers
带玻璃毛细管粘度计的手动运动粘度恒温浴
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润滑油低温旋转粘度计
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| Test method | ASTM D2983, ASTM D2196 |
|---|---|
| Temperature range | -40 to 20 °C |
| Temperature stability | ±0.1 °C |
| Viscosity range | 100–2,000,000 mPa·s with spindles |
| Spindle speed | 0.3–100 rpm |
| Torque accuracy | ±1% of full scale |
By Lab Manufacturers China Technical TeamLast reviewed Standards: ASTM D445, ISO 3104, ASTM D88
A low-temperature rotational viscometer measures apparent viscosity of gear oils, hydraulic fluids and transmission fluids by rotating a spindle in a cooled sample. It follows ASTM D2983, which reports Brookfield viscosity between -5 and -40 °C, and suits lubricant developers and quality laboratories.
A low-temperature rotational viscometer measures apparent viscosity of gear oils, hydraulic fluids and transmission fluids by rotating a spindle in a cooled sample. It follows ASTM D2983, which reports Brookfield viscosity between -5 and -40 °C, and suits lubricant developers and quality laboratories.
The low-temperature rotational viscometer combines a Brookfield-type rotational head with a cold bath or air-cooled chamber. A cylindrical spindle rotates in the sample at a defined speed, often 12 rpm, and the instrument measures the torque required to overcome viscous drag, which is converted to viscosity in mPa·s. In ASTM D2983, the sample is cooled in a bath to the test temperature between -5 and -40 °C for a fixed soak period, typically 16 hours, and then measured. Cooling may use a mechanical refrigerator or a cooled liquid circulator. The test suits low-temperature gear oils, automatic transmission fluids and hydraulic oils, for which apparent viscosity indicates pumpability and flow. Torque range should be selected so readings fall between 10 and 100 percent of full scale. Fluids with high shear sensitivity will show different values at different speeds, which is informative about non-Newtonian behavior.
Kinematic viscosity testers time the gravity-driven flow of a fixed liquid volume through a calibrated glass capillary viscometer held in a constant-temperature bath. Viscosity equals the measured flow time multiplied by the tube constant, expressed in mm²/s, and bath temperature must be held within about 0.02 °C because viscosity changes rapidly with temperature. Rotational instruments drive a spindle or rotor in the sample and measure the torque required, giving dynamic viscosity in mPa·s. Cold-cranking simulators rotate a rotor inside a stator at low temperature and relate motor speed to apparent viscosity for engine oils. Efflux cup methods such as Saybolt measure time for a set volume to drain through an orifice. Key components are the bath, thermostat, viscometer tubes, timing device and, in automatic models, optical or ultrasonic meniscus sensors.
A typical low-temperature rotational viscometer for lubricants configuration offers test method of ASTM D2983, ASTM D2196, temperature range of -40 to 20 °C, temperature stability of ±0.1 °C, viscosity range of 100–2,000,000 mPa·s with spindles, spindle speed of 0.3–100 rpm and torque accuracy of ±1% of full scale. Values are indicative of the product class; the exact figures for each configuration are confirmed on the quotation and the calibration documents supplied with the instrument.
The Low-Temperature Rotational Viscometer for Lubricants is used in gear oil low-temperature testing, automatic transmission fluid development, hydraulic oil pumpability and additive screening. Across the wider Viscosity Testers class, laboratories also deploy it for lubricant viscosity grade verification, fuel oil and diesel specification testing and engine oil low-temperature grading.
Relevant standards and methods include ASTM D445, ISO 3104, ASTM D88, ASTM D2983, ASTM D5293, SAE J300, IP 71, GB/T 265 and IEC 61010-1. Certification candidates for this model are CE and ISO 9001 manufacturing; each is to be confirmed for the specific configuration before shipment, and certificates are supplied only where they have been issued.
Level the bath and keep it away from drafts and vibration, because temperature stability and tube verticality drive precision. Use certified viscosity reference standards to calibrate tubes and check the bath thermometer against a traceable reference at least annually. Filter or degas samples to remove particles and bubbles, and allow adequate thermal equilibration, usually 15 to 30 minutes. Clean viscometer tubes with suitable solvents and dry with filtered air so residue does not change the tube constant. Inspect glass for cracks or chips. Replace bath fluid at intervals recommended by the supplier. For rotational and cold-cranking instruments, verify torque and speed calibration with standard oils and keep cooling systems free of moisture build-up.
Select this viscometer for low-temperature apparent viscosity of gear, transmission and hydraulic oils under D2983. For engine oil cranking viscosity, use a cold-cranking simulator instead. In an RFQ specify minimum temperature, spindle set, cooling method, torque range, data output needs, and whether a 16-hour cold soak bath is to be supplied.
Choose by the method named in your product specification. ASTM D445 capillary viscometry is the reference for kinematic viscosity of fuels and lubricants, and automatic multi-tube instruments raise throughput and remove timing subjectivity. Saybolt viscometers remain in use where legacy specifications are expressed in Saybolt seconds. Rotational instruments suit non-Newtonian or very viscous products and low-temperature lubricant tests, while cold-cranking simulators are specific to engine oil low-temperature grading under SAE J300. Consider the temperature range, from 40 and 100 °C for routine oils to -40 °C for low-temperature work, and confirm the bath can maintain stability. Check the tube range, sample volume, cleaning and drying arrangements, and calibration fluid availability. For large workloads, automatic cleaning stations and multi-position baths reduce labor considerably.
| Test method | ASTM D2983, ASTM D2196 |
|---|---|
| Temperature range | -40 to 20 °C |
| Temperature stability | ±0.1 °C |
| Viscosity range | 100–2,000,000 mPa·s with spindles |
| Spindle speed | 0.3–100 rpm |
| Torque accuracy | ±1% of full scale |
| Cooling | Mechanical refrigeration |
| Sample volume | About 40 mL |
| Data output | USB, printer |
| Power supply | 220 V, 50 Hz, 1500 W |
Indicative values for this product class. Final specifications are confirmed on the quotation and in the calibration documents supplied with the instrument.
ASTM D2983 measures low-shear-rate apparent viscosity of automatic transmission fluids, gear oils, hydraulic fluids and similar lubricants between -5 and -40 °C using a Brookfield-type rotational viscometer after a long cold soak.
The long soak, typically 16 hours, lets wax and structure form as they would during extended cold storage, so the measurement reflects realistic low-temperature behavior. Shorter soaking can underestimate viscosity in fluids that gel.
Yes, by changing spindle speed and recording torque, you can see how viscosity varies with shear rate. The result is apparent viscosity at the chosen conditions, so report spindle, speed and temperature with every value.
Kinematic viscosity is the flow time of a liquid under gravity, expressed in mm²/s, and equals dynamic viscosity divided by density. Dynamic viscosity is the resistance to shear measured by torque in rotational instruments, expressed in mPa·s. Fuel and lubricant specifications commonly use kinematic values.
Viscosity of oils changes by several percent per degree Celsius, so even small temperature errors create large errors in results. ASTM D445 requires bath stability within 0.02 °C at 40 and 100 °C, which needs a well-stirred thermostat and a calibrated reference thermometer.
Viscosity index is calculated from kinematic viscosity at 40 and 100 °C using the equations in ASTM D2270. A higher index means viscosity changes less with temperature. Lubricant suppliers report it to describe how oil behaves between cold start and operating temperature.

带玻璃毛细管粘度计的手动运动粘度恒温浴




